Implementing one-shot multiple-FID acquisition into homonuclear and heteronuclear NMR experiments

Kumar Motiram-Corral; Míriam Pérez-Trujillo; Pau Nolis; Teodor Parella

doi:10.1039/c8cc08065h

Implementing one-shot multiple-FID acquisition into homonuclear and heteronuclear NMR experiments

Kumar Motiram-Corral, Míriam Pérez-Trujillo, Pau Nolis, Teodor Parella

Producción científica: Contribución a una revista › Artículo › Investigación › revisión exhaustiva

14 Citas (Scopus)

Resumen

Multiple-FID acquisition (MFA) within the same scan is applied to acquire simultaneously multiple 2D spectra from a single NMR experiment. A discussion on the incorporation of the MFA strategy in several homonuclear and heteronuclear 2D pulse sequences is presented. As a proof of concept, a set of novel COSY, TOCSY and HMBC experiments are reported as a time-efficient solution in small-molecule NMR spectroscopy.

Idioma original	Inglés
Páginas (desde-hasta)	13507-13510
Número de páginas	4
Publicación	Chemical Communications
Volumen	54
N.º	96
DOI	https://doi.org/10.1039/c8cc08065h
Estado	Publicada - 2018

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Advances in NMR spectroscopic methodology and applications: time-efficient methods, ultra long-range heteronuclear correlation experiments and enantiospecific analysis of complex mixtures
Motiram Corral, K. (Autor/a)Parella Coll, T. (Director/a), Perez Trujillo, M. (Director/a), Nolis Fañanas, P. (Director/a) & Jaime Cardiel, C. (Tutor/a), 21 oct 2021
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abstract = "Multiple-FID acquisition (MFA) within the same scan is applied to acquire simultaneously multiple 2D spectra from a single NMR experiment. A discussion on the incorporation of the MFA strategy in several homonuclear and heteronuclear 2D pulse sequences is presented. As a proof of concept, a set of novel COSY, TOCSY and HMBC experiments are reported as a time-efficient solution in small-molecule NMR spectroscopy.",

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AU - Parella, Teodor

PY - 2018

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AB - Multiple-FID acquisition (MFA) within the same scan is applied to acquire simultaneously multiple 2D spectra from a single NMR experiment. A discussion on the incorporation of the MFA strategy in several homonuclear and heteronuclear 2D pulse sequences is presented. As a proof of concept, a set of novel COSY, TOCSY and HMBC experiments are reported as a time-efficient solution in small-molecule NMR spectroscopy.

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JO - Chemical Communications

JF - Chemical Communications

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Implementing one-shot multiple-FID acquisition into homonuclear and heteronuclear NMR experiments

Resumen

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Huella

Tesis doctorales

Advances in NMR spectroscopic methodology and applications: time-efficient methods, ultra long-range heteronuclear correlation experiments and enantiospecific analysis of complex mixtures

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