Time-shared NMR experiments

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Abstract

Details on the implementation of the simultaneous evolution of multiple frequencies into the same time period of a NMR pulse sequence are introduced. Timeshared (TS) versions of the most useful inverse 2D NMR experiments (TS-HMBC, TS-HSQC, TS-HSQC-TOCSY, and TS-HSQMBC) are presented and illustrated for simultaneous acquisition of 1H/13C and 1H/15N NMR spectra. The major benefits associated to the parallel acquisition of multiple spectra from a single NMR experiment are spectrometer time savings and the achievement of multiple and complementary information with improved sensitivity gains per time unit. © 2010 Wiley Periodicals, Inc.
Original languageEnglish
Pages (from-to)1-23
JournalConcepts in Magnetic Resonance Part A: Bridging Education and Research
Volume36
Issue number1
DOIs
Publication statusPublished - 14 May 2010

Keywords

  • Coupling constants
  • HMBC
  • HSQC
  • HSQC-TOCSY
  • HSQMBC
  • IPAP
  • Time-sharing

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