Synthesis, high-resolution NMR spectroscopic analysis, and single-crystal X-ray diffraction of isoxazoline tetracycles

Mirta L. Fascio, Angel Alvarez-Larena, Norma B. D'Accorso

    Research output: Contribution to journalArticleResearchpeer-review

    4 Citations (Scopus)

    Abstract

    Three isoxazoline tetracycles were obtained enantiomerically pure by intramolecular 1,3-dipolar cycloaddition. The characterization of the new compounds was performed by high-resolution 1H and 13C NMR spectroscopy. The relative configuration of the new chiral centers was determined by NOESY experiments and confirmed by single-crystal X-ray structural analysis. © 2002 Elsevier Science Ltd. All rights reserved.
    Original languageEnglish
    Pages (from-to)2419-2425
    JournalCarbohydrate Research
    Volume337
    Issue number24
    DOIs
    Publication statusPublished - 29 Nov 2002

    Keywords

    • Intramolecular 1,3-dipolar cycloaddition
    • Isoxazolines
    • Stereocontrol, NMR spectroscopy
    • X-Ray crystallography

    Fingerprint Dive into the research topics of 'Synthesis, high-resolution NMR spectroscopic analysis, and single-crystal X-ray diffraction of isoxazoline tetracycles'. Together they form a unique fingerprint.

    Cite this