Pure in-phase heteronuclear correlation NMR experiments

Laura Castañar, Josep Saurí, Robert Thomas Williamson, Albert Virgili, Teodor Parella

Research output: Contribution to journalArticleResearchpeer-review

29 Citations (Scopus)

Abstract

A general NMR approach to provide pure in-phase (PIP) multiplets in heteronuclear correlation experiments is described. The implementation of a zero-quantum filter efficiently suppresses any unwanted anti-phase contributions that usually distort the multiplet pattern of cross-peaks and can hamper their analysis. The clean pattern obtained in PIP-HSQMBC experiments is suitable for a direct extraction of coupling constants in resolved signals, for a peak-fitting process from a reference signal, and for the application of the IPAP technique in non-resolved multiplets. © 2014 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.
Original languageEnglish
Pages (from-to)8379-8382
JournalAngewandte Chemie - International Edition
Volume53
Issue number32
DOIs
Publication statusPublished - 4 Aug 2014

Keywords

  • coupling constants
  • heteronuclear long-range correlation
  • HSQC
  • HSQMBC
  • pure in-phase NMR

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