Preparation of homochiral 9-anthryl-tert-butylcarbinol. The configurational and conformational NMR study of its carbamate derivatives

Maria de Moragas, Adriana Port, Xavier Sánchez-Ruiz, Carlos Jaime, Christian Roussel, Albert Virgili

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9 Citations (Scopus)

Abstract

The homochiral carbamates of 9-anthryl-tert-butylcarbinol were prepared and their conformational equilibrium was studied. The absolute configuration was determined by comparison of the NMR data with MM calculations. The enantiomers of the alcohol were obtained after chromatographic separation of carbamate derivatives and their hydrolysis. The same homochiral alcohols were prepared by direct chiral column chromatography. © 1995.
Original languageEnglish
Pages (from-to)1307-1310
JournalTetrahedron: asymmetry
Volume6
Issue number6
DOIs
Publication statusPublished - 1 Jan 1995

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