Parametric aqueous electrodeposition study and characterization of Fe–Cu films

Evangelia Dislaki; Jordi Sort; Eva Pellicer

doi:https://doi.org/10.1016/j.electacta.2017.02.092

Parametric aqueous electrodeposition study and characterization of Fe–Cu films

Evangelia Dislaki, Jordi Sort, Eva Pellicer

Research output: Contribution to journal › Article › Research › peer-review

11 Citations (Scopus)

Abstract

© 2017 Elsevier Ltd In this study, FexCu1−x films over a wide composition range (0≤x≤86) were prepared from an aqueous sulfate electrolytic solution using three different complexing agents and variable plating conditions. The effect of parameters such as bath composition, current density and temperature on the elemental composition, morphology, structure and magnetic properties of the deposits was investigated. The electrochemical behavior was studied using cyclic voltammetry. High quality, smooth deposits with good substrate adhesion and minimized oxygen content were achieved. X-ray patterns indicate phase separation, though results from Rietveld analysis strongly suggest partial alloying. Magnetization dependence on Fe content is clearly demonstrated.

Original language	English
Pages (from-to)	739-748
Journal	Electrochimica Acta
Volume	231
DOIs	https://doi.org/10.1016/j.electacta.2017.02.092
Publication status	Published - 20 Mar 2017

Keywords

Co-deposition
Cu-based alloy
Electroplating
Fe-based alloy
Magnetic properties

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title = "Parametric aqueous electrodeposition study and characterization of Fe–Cu films",

abstract = "{\textcopyright} 2017 Elsevier Ltd In this study, FexCu1−x films over a wide composition range (0≤x≤86) were prepared from an aqueous sulfate electrolytic solution using three different complexing agents and variable plating conditions. The effect of parameters such as bath composition, current density and temperature on the elemental composition, morphology, structure and magnetic properties of the deposits was investigated. The electrochemical behavior was studied using cyclic voltammetry. High quality, smooth deposits with good substrate adhesion and minimized oxygen content were achieved. X-ray patterns indicate phase separation, though results from Rietveld analysis strongly suggest partial alloying. Magnetization dependence on Fe content is clearly demonstrated.",

keywords = "Co-deposition, Cu-based alloy, Electroplating, Fe-based alloy, Magnetic properties",

author = "Evangelia Dislaki and Jordi Sort and Eva Pellicer",

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T1 - Parametric aqueous electrodeposition study and characterization of Fe–Cu films

AU - Dislaki, Evangelia

AU - Sort, Jordi

AU - Pellicer, Eva

PY - 2017/3/20

Y1 - 2017/3/20

N2 - © 2017 Elsevier Ltd In this study, FexCu1−x films over a wide composition range (0≤x≤86) were prepared from an aqueous sulfate electrolytic solution using three different complexing agents and variable plating conditions. The effect of parameters such as bath composition, current density and temperature on the elemental composition, morphology, structure and magnetic properties of the deposits was investigated. The electrochemical behavior was studied using cyclic voltammetry. High quality, smooth deposits with good substrate adhesion and minimized oxygen content were achieved. X-ray patterns indicate phase separation, though results from Rietveld analysis strongly suggest partial alloying. Magnetization dependence on Fe content is clearly demonstrated.

AB - © 2017 Elsevier Ltd In this study, FexCu1−x films over a wide composition range (0≤x≤86) were prepared from an aqueous sulfate electrolytic solution using three different complexing agents and variable plating conditions. The effect of parameters such as bath composition, current density and temperature on the elemental composition, morphology, structure and magnetic properties of the deposits was investigated. The electrochemical behavior was studied using cyclic voltammetry. High quality, smooth deposits with good substrate adhesion and minimized oxygen content were achieved. X-ray patterns indicate phase separation, though results from Rietveld analysis strongly suggest partial alloying. Magnetization dependence on Fe content is clearly demonstrated.

KW - Co-deposition

KW - Cu-based alloy

KW - Electroplating

KW - Fe-based alloy

KW - Magnetic properties

U2 - https://doi.org/10.1016/j.electacta.2017.02.092

DO - https://doi.org/10.1016/j.electacta.2017.02.092

M3 - Article

VL - 231

SP - 739

EP - 748

JO - Electrochimica Acta

JF - Electrochimica Acta

SN - 0013-4686

ER -