Novel [1n]-meta-heterophane frameworks with a bis-betaine nature

E. Alcalde, C. Ayala, I. Dinarès, N. Mesquida, F. Sánchez-Ferrando

Research output: Contribution to journalArticleResearchpeer-review

13 Citations (Scopus)

Abstract

A convergent "5 + 1" and "5 + 3" synthetic strategy allowed the synthesis of the first examples of bis-betaines 2 and 3, a prototype of phanes that incorporate heterocyclic betaines. The structure of the quadrupolar macrocyclic systems 2 and 3 together with the dicationic [16]- and [18] meta-heterophane precursors 5•2X and 6•2X were examined by spectroscopy using 1H and 13C NMR techniques together with 1H-DNMR studies and electrospray ionization mass spectrometry.
Original languageEnglish
Pages (from-to)2281-2290
JournalJournal of Organic Chemistry
Volume66
Issue number7
DOIs
Publication statusPublished - 6 Apr 2001

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