Multiple FID acquisition of complementary HMBC data

Pau Nolis; Miriam Pérez-Trujillo; Teodor Parella

doi:10.1002/anie.200702258

Multiple FID acquisition of complementary HMBC data

Pau Nolis, Miriam Pérez-Trujillo, Teodor Parella

Department of Chemistry

Research output: Contribution to journal › Article › Research › peer-review

24 Citations (Scopus)

Abstract

(Figure Presented) One experiment, four NMR spectra: By combining the principles of time-sharing evolution and multiple FID acquisition within the same scan, several fully complementary NMR spectra can be obtained in a single-shot acquisition. Four different HMBC and HMBC-relayed experiments (see spectra) can be carried out simultaneously for 13C and 15N at natural abundance, with a saving in measuring time of up to 75%. © 2007 Wiley-VCH Verlag GmbH & Co. KGaA.

Original language	English
Pages (from-to)	7495-7497
Journal	Angewandte Chemie - International Edition
Volume	46
Issue number	39
DOIs	https://doi.org/10.1002/anie.200702258
Publication status	Published - 16 Oct 2007

Keywords

HMBC spectroscopy
Multiple acquisition
NMR spectroscopy
Structure determination
Time-sharing evolution

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abstract = "(Figure Presented) One experiment, four NMR spectra: By combining the principles of time-sharing evolution and multiple FID acquisition within the same scan, several fully complementary NMR spectra can be obtained in a single-shot acquisition. Four different HMBC and HMBC-relayed experiments (see spectra) can be carried out simultaneously for 13C and 15N at natural abundance, with a saving in measuring time of up to 75%. {\textcopyright} 2007 Wiley-VCH Verlag GmbH & Co. KGaA.",

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AU - Nolis, Pau

AU - Pérez-Trujillo, Miriam

AU - Parella, Teodor

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N2 - (Figure Presented) One experiment, four NMR spectra: By combining the principles of time-sharing evolution and multiple FID acquisition within the same scan, several fully complementary NMR spectra can be obtained in a single-shot acquisition. Four different HMBC and HMBC-relayed experiments (see spectra) can be carried out simultaneously for 13C and 15N at natural abundance, with a saving in measuring time of up to 75%. © 2007 Wiley-VCH Verlag GmbH & Co. KGaA.

AB - (Figure Presented) One experiment, four NMR spectra: By combining the principles of time-sharing evolution and multiple FID acquisition within the same scan, several fully complementary NMR spectra can be obtained in a single-shot acquisition. Four different HMBC and HMBC-relayed experiments (see spectra) can be carried out simultaneously for 13C and 15N at natural abundance, with a saving in measuring time of up to 75%. © 2007 Wiley-VCH Verlag GmbH & Co. KGaA.

KW - HMBC spectroscopy

KW - Multiple acquisition

KW - NMR spectroscopy

KW - Structure determination

KW - Time-sharing evolution

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DO - 10.1002/anie.200702258

M3 - Article

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SP - 7495

EP - 7497

JO - Angewandte Chemie - International Edition

JF - Angewandte Chemie - International Edition

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