Influence of the milling conditions on the amorphization of Fe<inf>82</inf>Nb<inf>6</inf>B<inf>12</inf> alloy

Z. Caamaño, G. Pérez, L. E. Zamora, S. Suriñach, J. S. Muñoz, M. D. Baró

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Abstract

Fe82Nb6B12 alloy was synthesized from the elemental powders by a planetary high-energy ball mill, at room temperature, using different milling times and different surfactants. The products were measured by X-ray diffraction, magnetic thermogravimetry, vibrating sample magnetometer, and Mössbauer spectroscopy. Amorphization was observed from the X-ray diffraction on a sample ball milled for about 220 h using 595 rpm and cyclohexane as surfactant. Nevertheless, using the same conditions without surfactant, only the bcc Fe was found. The results are compared with data for rapidly quenched materials. © 2001 Elsevier Science B.V. All rights reserved.
Original languageEnglish
Pages (from-to)15-19
JournalJournal of Non-Crystalline Solids
Volume287
DOIs
Publication statusPublished - 1 Jul 2001

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