Improved multiplicity-edited ADEQUATE experiments

Teodor Parella; Francesc Sánchez-Ferrando

doi:10.1016/j.jmr.2003.10.010

Improved multiplicity-edited ADEQUATE experiments

Teodor Parella, Francesc Sánchez-Ferrando

Department of Chemistry

Research output: Contribution to journal › Article › Research › peer-review

16 Citations (Scopus)

Abstract

The use of ADEQUATE spectrum to extract carbon-carbon connectivities along with the carbon multiplicity was discussed. The spectrum correlates the spin systems by displaying proton chemical shift and double quantum carbon frequencies in the pulses. The results show the simultaneous achievement of the carbon multiplicity information and the chemical shift assignments. The comparison between the performance of pulse schemes and the transfer efficiencies for different spin systems was also discussed.

Original language	English
Pages (from-to)	123-128
Journal	Journal of Magnetic Resonance
Volume	166
Issue number	1
DOIs	https://doi.org/10.1016/j.jmr.2003.10.010
Publication status	Published - 1 Jan 2004

Keywords

2D NMR
Adequate
Carbon multiplicity
NMR

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10.1016/j.jmr.2003.10.010

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title = "Improved multiplicity-edited ADEQUATE experiments",

abstract = "The use of ADEQUATE spectrum to extract carbon-carbon connectivities along with the carbon multiplicity was discussed. The spectrum correlates the spin systems by displaying proton chemical shift and double quantum carbon frequencies in the pulses. The results show the simultaneous achievement of the carbon multiplicity information and the chemical shift assignments. The comparison between the performance of pulse schemes and the transfer efficiencies for different spin systems was also discussed.",

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AU - Sánchez-Ferrando, Francesc

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N2 - The use of ADEQUATE spectrum to extract carbon-carbon connectivities along with the carbon multiplicity was discussed. The spectrum correlates the spin systems by displaying proton chemical shift and double quantum carbon frequencies in the pulses. The results show the simultaneous achievement of the carbon multiplicity information and the chemical shift assignments. The comparison between the performance of pulse schemes and the transfer efficiencies for different spin systems was also discussed.

AB - The use of ADEQUATE spectrum to extract carbon-carbon connectivities along with the carbon multiplicity was discussed. The spectrum correlates the spin systems by displaying proton chemical shift and double quantum carbon frequencies in the pulses. The results show the simultaneous achievement of the carbon multiplicity information and the chemical shift assignments. The comparison between the performance of pulse schemes and the transfer efficiencies for different spin systems was also discussed.

KW - 2D NMR

KW - Adequate

KW - Carbon multiplicity

KW - NMR

U2 - 10.1016/j.jmr.2003.10.010

DO - 10.1016/j.jmr.2003.10.010

M3 - Article

VL - 166

SP - 123

EP - 128

IS - 1

ER -

Improved multiplicity-edited ADEQUATE experiments

Abstract

Keywords

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