Implementing multiplicity editing in selective HSQMBC experiments

Josep Saurí, Eduard Sistaré, R. Thomas Williamson, Gary E. Martin, Teodor Parella

    Research output: Contribution to journalArticleResearchpeer-review

    9 Citations (Scopus)

    Abstract

    © 2015 Elsevier Inc. All rights reserved. Even C/CH2 and odd CH/CH3 carbon-multiplicity information can be directly distinguished from the relative positive/negative phase of cross-peaks in a novel ME (Multiplicity-Edited)-selHSQMBC experiment. The method can be extended by a TOCSY propagation step, and it is fully compatible for the simultaneous and precise determination of long-range heteronuclear coupling constants. Broadband homonuclear decoupling techniques can also be incorporated to enhance sensitivity and signal resolution by effective collapse of J(HH) multiplets.
    Original languageEnglish
    Pages (from-to)170-175
    JournalJournal of Magnetic Resonance
    Volume252
    DOIs
    Publication statusPublished - 1 Jan 2015

    Keywords

    • Heteronuclear coupling constants
    • HOBS
    • HSQMBC
    • IPAP
    • Multiplicity-editing

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