Full sensitivity and enhanced resolution in homodecoupled band-selective NMR experiments

Laura Castañar; Pau Nolis; Albert Virgili; Teodor Parella

doi:10.1002/chem.201303235

Full sensitivity and enhanced resolution in homodecoupled band-selective NMR experiments

Laura Castañar, Pau Nolis, Albert Virgili, Teodor Parella

Department of Chemistry

Research output: Contribution to journal › Article › Research › peer-review

95 Citations (Scopus)

Abstract

Fingers on the pulse: An NMR pulse scheme that provides full sensitivity in homodecoupled band-selective NMR spectroscopy experiments is proposed (see figure). The easy implementation of this HOBS scheme as a general building block into a great variety of multidimensional NMR experiments leads to pure-shift spectra with enhanced resolution and with the maximum attainable sensitivity. © 2013 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

Original language	English
Pages (from-to)	17283-17286
Journal	Chemistry - A European Journal
Volume	19
Issue number	51
DOIs	https://doi.org/10.1002/chem.201303235
Publication status	Published - 16 Dec 2013

Keywords

band selective
homodecoupling
NMR spectroscopy
sensitivity enhancement
structure elucidation

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abstract = "Fingers on the pulse: An NMR pulse scheme that provides full sensitivity in homodecoupled band-selective NMR spectroscopy experiments is proposed (see figure). The easy implementation of this HOBS scheme as a general building block into a great variety of multidimensional NMR experiments leads to pure-shift spectra with enhanced resolution and with the maximum attainable sensitivity. {\textcopyright} 2013 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.",

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AU - Nolis, Pau

AU - Virgili, Albert

AU - Parella, Teodor

PY - 2013/12/16

Y1 - 2013/12/16

N2 - Fingers on the pulse: An NMR pulse scheme that provides full sensitivity in homodecoupled band-selective NMR spectroscopy experiments is proposed (see figure). The easy implementation of this HOBS scheme as a general building block into a great variety of multidimensional NMR experiments leads to pure-shift spectra with enhanced resolution and with the maximum attainable sensitivity. © 2013 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

AB - Fingers on the pulse: An NMR pulse scheme that provides full sensitivity in homodecoupled band-selective NMR spectroscopy experiments is proposed (see figure). The easy implementation of this HOBS scheme as a general building block into a great variety of multidimensional NMR experiments leads to pure-shift spectra with enhanced resolution and with the maximum attainable sensitivity. © 2013 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

KW - band selective

KW - homodecoupling

KW - NMR spectroscopy

KW - sensitivity enhancement

KW - structure elucidation

U2 - 10.1002/chem.201303235

DO - 10.1002/chem.201303235

M3 - Article

VL - 19

SP - 17283

EP - 17286

IS - 51

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Full sensitivity and enhanced resolution in homodecoupled band-selective NMR experiments

Abstract

Keywords

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