Crystal structure and spectroscopic study of methyl (Z)-6-anilino-4-cyano-2,3-dimethoxy-6-azapentafulvene-1-carboxylate

J. F. Piniella; J. Rius; A. Alvarez-Larena; X. Batllori; P. Victory

doi:10.1007/BF01160664

Crystal structure and spectroscopic study of methyl (Z)-6-anilino-4-cyano-2,3-dimethoxy-6-azapentafulvene-1-carboxylate

J. F. Piniella, J. Rius, A. Alvarez-Larena, X. Batllori, P. Victory

Department of Geology

Research output: Contribution to journal › Article › Research › peer-review

2 Citations (Scopus)

Abstract

The molecular and crystal structures of the title compound have been determined. The crystals are monoclinic: C2/c (15), a=21.787(7), b=7.025(6), c=20.165(8) Å, β=96.03(2)°, Vc =3069 Å3, Z=8, Dx=1.36 mg m-3, λ=(Mo K α)=0.71069 Å. The structure was solved by direct methods and refined with 1484 reflections to a final R value of 0.057. Mass and spectral data (ir, uv,1H and13C nmr) are also reported. The structure appears to be polyolefinic having two independent push-pull systems on the fulvenic ring. © 1991 Plenum Publishing Corporation.

Original language	English
Pages (from-to)	489-494
Journal	Journal of Crystallographic and Spectroscopic Research
Volume	21
Issue number	4
DOIs	https://doi.org/10.1007/BF01160664
Publication status	Published - 1 Aug 1991

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@article{60e4af55f7444d01ac0ff72a4e9b84da,

title = "Crystal structure and spectroscopic study of methyl (Z)-6-anilino-4-cyano-2,3-dimethoxy-6-azapentafulvene-1-carboxylate",

abstract = "The molecular and crystal structures of the title compound have been determined. The crystals are monoclinic: C2/c (15), a=21.787(7), b=7.025(6), c=20.165(8) {\AA}, β=96.03(2)°, Vc =3069 {\AA}3, Z=8, Dx=1.36 mg m-3, λ=(Mo K α)=0.71069 {\AA}. The structure was solved by direct methods and refined with 1484 reflections to a final R value of 0.057. Mass and spectral data (ir, uv,1H and13C nmr) are also reported. The structure appears to be polyolefinic having two independent push-pull systems on the fulvenic ring. {\textcopyright} 1991 Plenum Publishing Corporation.",

author = "Piniella, {J. F.} and J. Rius and A. Alvarez-Larena and X. Batllori and P. Victory",

year = "1991",

month = aug,

day = "1",

doi = "10.1007/BF01160664",

language = "English",

volume = "21",

pages = "489--494",

number = "4",

}

TY - JOUR

T1 - Crystal structure and spectroscopic study of methyl (Z)-6-anilino-4-cyano-2,3-dimethoxy-6-azapentafulvene-1-carboxylate

AU - Piniella, J. F.

AU - Rius, J.

AU - Alvarez-Larena, A.

AU - Batllori, X.

AU - Victory, P.

PY - 1991/8/1

Y1 - 1991/8/1

N2 - The molecular and crystal structures of the title compound have been determined. The crystals are monoclinic: C2/c (15), a=21.787(7), b=7.025(6), c=20.165(8) Å, β=96.03(2)°, Vc =3069 Å3, Z=8, Dx=1.36 mg m-3, λ=(Mo K α)=0.71069 Å. The structure was solved by direct methods and refined with 1484 reflections to a final R value of 0.057. Mass and spectral data (ir, uv,1H and13C nmr) are also reported. The structure appears to be polyolefinic having two independent push-pull systems on the fulvenic ring. © 1991 Plenum Publishing Corporation.

AB - The molecular and crystal structures of the title compound have been determined. The crystals are monoclinic: C2/c (15), a=21.787(7), b=7.025(6), c=20.165(8) Å, β=96.03(2)°, Vc =3069 Å3, Z=8, Dx=1.36 mg m-3, λ=(Mo K α)=0.71069 Å. The structure was solved by direct methods and refined with 1484 reflections to a final R value of 0.057. Mass and spectral data (ir, uv,1H and13C nmr) are also reported. The structure appears to be polyolefinic having two independent push-pull systems on the fulvenic ring. © 1991 Plenum Publishing Corporation.

U2 - 10.1007/BF01160664

DO - 10.1007/BF01160664

M3 - Article

VL - 21

SP - 489

EP - 494

IS - 4

ER -

Crystal structure and spectroscopic study of methyl (Z)-6-anilino-4-cyano-2,3-dimethoxy-6-azapentafulvene-1-carboxylate

Abstract

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