Composition of iodopropylideneglycerol: An example of the application of 2D NMR spectroscopy to structure elucidation

A. Virgili, J. Cervelló

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Abstract

Using 1D and 2D NMR spectra, the compounds obtained, in a mixture, in the reaction of glycerol with iodine were identified as the two isomers (cis and trans) of 2-iodomethyl-5-hydroxymethyl-1,4-dioxane and the two isomers (cis and trans) of 2-iodomethyl-6-hydroxymethyl-1,4-dioxane. Thus, the composition of the pharmaceutical formulation named IPG has finally been established.
Original languageEnglish
Pages (from-to)434-439
JournalMagnetic Resonance in Chemistry
Volume34
Issue number6
DOIs
Publication statusPublished - 1 Jun 1996

Keywords

  • 13 C NMR
  • 1 H NMR
  • Dioxanes
  • Gradient-enhanced 2D NMR
  • Iodopropylideneglycerol

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