X-ray, IR and 1H-NMR structural and conformational study of highly congested 2-alkyl-1,3-diols and of 3-(1-adamantyl)pentane-2,4-dione

M. Moreno-Mañas, J. F. Piniella, A. Alvarez-Larena, N. Galvez, M. E. Lloris, J. Marquet, A. C. Siani, G. Germain

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Resum

Configuration of meso diols produced by LiA1H4 reduction of symmetric α-(1-adamantyl)-β-diketones has been determined by X-ray diffraction. Large C-C distances and C-C-C angles have been measured for these strained molecules. Most of the studied 1,3-diols, both meso and d,1, exist in solution in conformations possesing intramolecular hydrogen bond. The conformations of two diols were also studied in the crystal phase. © 1992.
Idioma originalAnglès
Pàgines (de-a)3611-3622
RevistaTetrahedron
Volum48
Número17
DOIs
Estat de la publicacióPublicada - 1 de gen. 1992

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