Use of selective heteronuclear 13c1h noe measurements. a second note of warning on the assignment of structure to the products formed in the reactions between 4-hydroxy-2h-pyran-2-ones and carbonyl compounds.

J. Cervello; M. Gil; P. de March; J. Marquet; M. Moreno-Mañas; J. L. Roca; F. Sanchez-Ferrando

doi:10.1016/S0040-4020(01)86824-1

Use of selective heteronuclear ¹³c¹h noe measurements. a second note of warning on the assignment of structure to the products formed in the reactions between 4-hydroxy-2h-pyran-2-ones and carbonyl compounds.

J. Cervello, M. Gil, P. de March, J. Marquet, M. Moreno-Mañas, J. L. Roca, F. Sanchez-Ferrando

Departament de Química

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17 Cites (Scopus)

Resum

Further examples of the occurrence of intramolecular translactonization during condensation of 4-hydroxy-6-methyl-2H-pyran-2-one, 1, or 4-hydroxycoumarin, 4, with carbonyl compounds are desoribed. The structure of previously misassigned products 6a,b is proven by NMR techniques. Application of the HETNOE method to the distinction between structures 9 and 10 is demonstrated. © 1987.

Idioma original	Anglès
Pàgines (de-a)	2381-2387
Revista	Tetrahedron
Volum	43
Número	10
DOIs	https://doi.org/10.1016/S0040-4020(01)86824-1
Estat de la publicació	Publicada - 1 de gen. 1987

Accés al document

10.1016/S0040-4020(01)86824-1

Altres arxius i enllaços

https://www.scopus.com/pages/publications/0001919493

Com citar-ho

Cervello, J., Gil, M., de March, P., Marquet, J., Moreno-Mañas, M., Roca, J. L., & Sanchez-Ferrando, F. (1987). Use of selective heteronuclear ¹³c¹h noe measurements. a second note of warning on the assignment of structure to the products formed in the reactions between 4-hydroxy-2h-pyran-2-ones and carbonyl compounds. Tetrahedron, 43(10), 2381-2387. https://doi.org/10.1016/S0040-4020(01)86824-1

@article{8950f0ceb623495988e682ff91e2d458,

title = "Use of selective heteronuclear 13c1h noe measurements. a second note of warning on the assignment of structure to the products formed in the reactions between 4-hydroxy-2h-pyran-2-ones and carbonyl compounds.",

abstract = "Further examples of the occurrence of intramolecular translactonization during condensation of 4-hydroxy-6-methyl-2H-pyran-2-one, 1, or 4-hydroxycoumarin, 4, with carbonyl compounds are desoribed. The structure of previously misassigned products 6a,b is proven by NMR techniques. Application of the HETNOE method to the distinction between structures 9 and 10 is demonstrated. {\textcopyright} 1987.",

author = "J. Cervello and M. Gil and \{de March\}, P. and J. Marquet and M. Moreno-Ma{\~n}as and Roca, \{J. L.\} and F. Sanchez-Ferrando",

year = "1987",

month = jan,

day = "1",

doi = "10.1016/S0040-4020(01)86824-1",

language = "English",

volume = "43",

pages = "2381--2387",

journal = "Tetrahedron",

issn = "0040-4020",

publisher = "Elsevier Limited",

number = "10",

}

Cervello, J, Gil, M, de March, P, Marquet, J, Moreno-Mañas, M, Roca, JL & Sanchez-Ferrando, F 1987, 'Use of selective heteronuclear ¹³c¹h noe measurements. a second note of warning on the assignment of structure to the products formed in the reactions between 4-hydroxy-2h-pyran-2-ones and carbonyl compounds.', Tetrahedron, vol. 43, núm. 10, pàg. 2381-2387. https://doi.org/10.1016/S0040-4020(01)86824-1

Use of selective heteronuclear ¹³c¹h noe measurements. a second note of warning on the assignment of structure to the products formed in the reactions between 4-hydroxy-2h-pyran-2-ones and carbonyl compounds. / Cervello, J.; Gil, M.; de March, P. et al.
In: Tetrahedron, Vol. 43, Núm. 10, 01.01.1987, pàg. 2381-2387.

Producció científica: Contribució a revista › Article › Recerca › Avaluat per experts

TY - JOUR

T1 - Use of selective heteronuclear 13c1h noe measurements. a second note of warning on the assignment of structure to the products formed in the reactions between 4-hydroxy-2h-pyran-2-ones and carbonyl compounds.

AU - Cervello, J.

AU - Gil, M.

AU - de March, P.

AU - Marquet, J.

AU - Moreno-Mañas, M.

AU - Roca, J. L.

AU - Sanchez-Ferrando, F.

PY - 1987/1/1

Y1 - 1987/1/1

N2 - Further examples of the occurrence of intramolecular translactonization during condensation of 4-hydroxy-6-methyl-2H-pyran-2-one, 1, or 4-hydroxycoumarin, 4, with carbonyl compounds are desoribed. The structure of previously misassigned products 6a,b is proven by NMR techniques. Application of the HETNOE method to the distinction between structures 9 and 10 is demonstrated. © 1987.

AB - Further examples of the occurrence of intramolecular translactonization during condensation of 4-hydroxy-6-methyl-2H-pyran-2-one, 1, or 4-hydroxycoumarin, 4, with carbonyl compounds are desoribed. The structure of previously misassigned products 6a,b is proven by NMR techniques. Application of the HETNOE method to the distinction between structures 9 and 10 is demonstrated. © 1987.

UR - https://www.scopus.com/pages/publications/0001919493

U2 - 10.1016/S0040-4020(01)86824-1

DO - 10.1016/S0040-4020(01)86824-1

M3 - Article

SN - 0040-4020

VL - 43

SP - 2381

EP - 2387

JO - Tetrahedron

JF - Tetrahedron

IS - 10