One step preparation and 1,3-dipolar cycloadditions of (S)-5-hydroxymethyl-1-pyrroline N-oxide

Montserrat Closa, Pedro De March, Marta Figueredo, Josep Font

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Resum

The cyclic nitrone 1b has been prepared in enantiomerically pure form by direct oxidation of L-(+)-prolinol with dimethyldioxirane. A complete diastereoface differentiation has been observed in the 1,3-dipolar cycloaddition reaction of this nitrone to several 1,2-disubstituted electron deficient olefins.
Idioma originalEnglish
Pàgines (de-a)1031-1037
RevistaTetrahedron Asymmetry
Volum8
Número7
DOIs
Estat de la publicacióPublicada - 11 d’abr. 1997

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