TY - JOUR
T1 - Improving the quality of XAFS data
AU - Abe, Hitoshi
AU - Aquilanti, Giuliana
AU - Boada, Roberto
AU - Bunker, Bruce
AU - Glatzel, Pieter
AU - Nachtegaal, Maarten
AU - Pascarelli, Sakura
N1 - Publisher Copyright:
© Hitoshi Abe et al. 2018
PY - 2018/7
Y1 - 2018/7
N2 - Following the Q2XAFS Workshop and Satellite to IUCr Congress 2017 on `Data Acquisition, Treatment, Storage – quality assurance in XAFS spectroscopy', a summary is given of the discussion on different aspects of a XAFS experiment that affect data quality. Some pertinent problems ranging from sources and minimization of noise to harmonic contamination and uncompensated monochromator glitches were addressed. Also, an overview is given of the major limitations and pitfalls of a selection of related methods, such as photon-out spectroscopies and energy-dispersive XAFS, and of increasingly common applications, namely studies at high pressure, and time-resolved investigations of catalysts in operando. Advice on how to avoid or deal with these problems and a few good practice recommendations are reported, including how to correctly report results.
AB - Following the Q2XAFS Workshop and Satellite to IUCr Congress 2017 on `Data Acquisition, Treatment, Storage – quality assurance in XAFS spectroscopy', a summary is given of the discussion on different aspects of a XAFS experiment that affect data quality. Some pertinent problems ranging from sources and minimization of noise to harmonic contamination and uncompensated monochromator glitches were addressed. Also, an overview is given of the major limitations and pitfalls of a selection of related methods, such as photon-out spectroscopies and energy-dispersive XAFS, and of increasingly common applications, namely studies at high pressure, and time-resolved investigations of catalysts in operando. Advice on how to avoid or deal with these problems and a few good practice recommendations are reported, including how to correctly report results.
KW - good practice in XAFS experiments
KW - harmonic rejection in XAFS
KW - quality of XAFS data
KW - sources of noise in XAFS
KW - XAFS
UR - http://www.scopus.com/inward/record.url?scp=85049587390&partnerID=8YFLogxK
U2 - 10.1107/S1600577518006021
DO - 10.1107/S1600577518006021
M3 - Article
C2 - 29979158
AN - SCOPUS:85049587390
SN - 0909-0495
VL - 25
SP - 972
EP - 980
JO - Journal of Synchrotron Radiation
JF - Journal of Synchrotron Radiation
IS - 4
ER -