Implementing one-shot multiple-FID acquisition into homonuclear and heteronuclear NMR experiments

Kumar Motiram-Corral; Míriam Pérez-Trujillo; Pau Nolis; Teodor Parella

doi:10.1039/c8cc08065h

Implementing one-shot multiple-FID acquisition into homonuclear and heteronuclear NMR experiments

Kumar Motiram-Corral, Míriam Pérez-Trujillo, Pau Nolis, Teodor Parella

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Resum

Multiple-FID acquisition (MFA) within the same scan is applied to acquire simultaneously multiple 2D spectra from a single NMR experiment. A discussion on the incorporation of the MFA strategy in several homonuclear and heteronuclear 2D pulse sequences is presented. As a proof of concept, a set of novel COSY, TOCSY and HMBC experiments are reported as a time-efficient solution in small-molecule NMR spectroscopy.

Idioma original	English
Pàgines (de-a)	13507-13510
Nombre de pàgines	4
Revista	Chemical Communications
Volum	54
Número	96
DOIs	https://doi.org/10.1039/c8cc08065h
Estat de la publicació	Publicada - 2018

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10.1039/c8cc08065h

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Advances in NMR spectroscopic methodology and applications: time-efficient methods, ultra long-range heteronuclear correlation experiments and enantiospecific analysis of complex mixtures
Motiram Corral, K. (Autor/a)Parella Coll, T. (Director/a), Perez Trujillo, M. (Director/a), Nolis Fañanas, P. (Director/a) & Jaime Cardiel, C. (Tutor/a), 21 d’oct. 2021
Tesi d’estudis: Tesi doctoral

Com citar-ho

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title = "Implementing one-shot multiple-FID acquisition into homonuclear and heteronuclear NMR experiments",

abstract = "Multiple-FID acquisition (MFA) within the same scan is applied to acquire simultaneously multiple 2D spectra from a single NMR experiment. A discussion on the incorporation of the MFA strategy in several homonuclear and heteronuclear 2D pulse sequences is presented. As a proof of concept, a set of novel COSY, TOCSY and HMBC experiments are reported as a time-efficient solution in small-molecule NMR spectroscopy.",

author = "Kumar Motiram-Corral and M{\'i}riam P{\'e}rez-Trujillo and Pau Nolis and Teodor Parella",

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T1 - Implementing one-shot multiple-FID acquisition into homonuclear and heteronuclear NMR experiments

AU - Motiram-Corral, Kumar

AU - Pérez-Trujillo, Míriam

AU - Nolis, Pau

AU - Parella, Teodor

PY - 2018

Y1 - 2018

N2 - Multiple-FID acquisition (MFA) within the same scan is applied to acquire simultaneously multiple 2D spectra from a single NMR experiment. A discussion on the incorporation of the MFA strategy in several homonuclear and heteronuclear 2D pulse sequences is presented. As a proof of concept, a set of novel COSY, TOCSY and HMBC experiments are reported as a time-efficient solution in small-molecule NMR spectroscopy.

AB - Multiple-FID acquisition (MFA) within the same scan is applied to acquire simultaneously multiple 2D spectra from a single NMR experiment. A discussion on the incorporation of the MFA strategy in several homonuclear and heteronuclear 2D pulse sequences is presented. As a proof of concept, a set of novel COSY, TOCSY and HMBC experiments are reported as a time-efficient solution in small-molecule NMR spectroscopy.

UR - http://www.scopus.com/inward/record.url?scp=85057450743&partnerID=8YFLogxK

U2 - 10.1039/c8cc08065h

DO - 10.1039/c8cc08065h

M3 - Article

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SN - 1359-7345

VL - 54

SP - 13507

EP - 13510

JO - Chemical Communications

JF - Chemical Communications

IS - 96

ER -

Implementing one-shot multiple-FID acquisition into homonuclear and heteronuclear NMR experiments

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Tesis doctorals

Advances in NMR spectroscopic methodology and applications: time-efficient methods, ultra long-range heteronuclear correlation experiments and enantiospecific analysis of complex mixtures

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