TY - JOUR
T1 - Effective multiple-solvent suppression scheme using the excitation sculpting principle
AU - Parella, Teodor
AU - Adell, Pere
AU - Sánchez-Ferrando, Francisco
AU - Virgili, Albert
PY - 1998/4/1
Y1 - 1998/4/1
N2 - An interesting and simple approach to effective multiple-solvent suppression is proposed using the basic principles of the excitation sculpting methodology. Flat baseline and ultra-clean NMR spectra are usually obtained under standard conditions using a modified double pulsed field gradient echo scheme in samples containing mixtures of non-deuterated solvents. The simple performance of such an approach, the high tolerance to experimental mis-settings, the impressive level of solvent suppression and the easy incorporation of the proposed scheme in multi-dimensional NMR experiments make this method suitable for possible applications in liquid chromatography NMR. © 1998 John Wiley & Sons, Ltd.
AB - An interesting and simple approach to effective multiple-solvent suppression is proposed using the basic principles of the excitation sculpting methodology. Flat baseline and ultra-clean NMR spectra are usually obtained under standard conditions using a modified double pulsed field gradient echo scheme in samples containing mixtures of non-deuterated solvents. The simple performance of such an approach, the high tolerance to experimental mis-settings, the impressive level of solvent suppression and the easy incorporation of the proposed scheme in multi-dimensional NMR experiments make this method suitable for possible applications in liquid chromatography NMR. © 1998 John Wiley & Sons, Ltd.
KW - Excitation sculpting
KW - Liquid chromatography
KW - Multiple solvent suppression
KW - NMR
KW - Pulsed field gradient
U2 - 10.1002/(SICI)1097-458X(199804)36:4<245::AID-OMR264>3.0.CO;2-J
DO - 10.1002/(SICI)1097-458X(199804)36:4<245::AID-OMR264>3.0.CO;2-J
M3 - Article
SN - 0749-1581
VL - 36
SP - 245
EP - 249
JO - Magnetic Resonance in Chemistry
JF - Magnetic Resonance in Chemistry
IS - 4
ER -