TY - JOUR
T1 - Composition of iodopropylideneglycerol: an Example of the Application of 2D NMR spectroscopy to Structure Elucidation
AU - Virgili, A.
AU - Cervelló, J.
PY - 1996/6/1
Y1 - 1996/6/1
N2 - Using 1D and 2D NMR spectra, the compounds obtained, in a mixture, in the reaction of glycerol with iodine were identified as the two isomers (cis and trans) of 2-iodomethyl-5-hydroxymethyl-1,4-dioxane and the two isomers (cis and trans) of 2-iodomethyl-6-hydroxymethyl-1,4-dioxane. Thus, the composition of the pharmaceutical formulation named IPG has finally been established.
AB - Using 1D and 2D NMR spectra, the compounds obtained, in a mixture, in the reaction of glycerol with iodine were identified as the two isomers (cis and trans) of 2-iodomethyl-5-hydroxymethyl-1,4-dioxane and the two isomers (cis and trans) of 2-iodomethyl-6-hydroxymethyl-1,4-dioxane. Thus, the composition of the pharmaceutical formulation named IPG has finally been established.
KW - 13 C NMR
KW - 1 H NMR
KW - Dioxanes
KW - Gradient-enhanced 2D NMR
KW - Iodopropylideneglycerol
UR - https://www.scopus.com/pages/publications/0030536564
U2 - 10.1002/(SICI)1097-458X(199606)34:6<434::AID-OMR897>3.0.CO;2-O
DO - 10.1002/(SICI)1097-458X(199606)34:6<434::AID-OMR897>3.0.CO;2-O
M3 - Article
SN - 0749-1581
VL - 34
SP - 434
EP - 439
JO - Magnetic Resonance in Chemistry
JF - Magnetic Resonance in Chemistry
IS - 6
ER -