Bis(η5-hydropentalenyl)iron

Elies Molins, Waldemar Maniukiewicz, Carlos Miravitlles, Montse Mas, Juan M. Manriquez, Ivonne Chavez, Beatriz Oelckers, Joan Farran, José Luis Briansó

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Resum

In the structure of bis[(3a,4,5,6,6a-η)-1-hydropentalenyl]iron, [Fe(C8H7)2], the two pentalene ligands are parallel. The molecules are packed in chains along the a axis and there are no significant intermolecular interactions. The compound shows disorder at the iron position with a 93.3% major and a 6.7% minor component. The structure of the predominant component has been determined. In addition, the double bond in one pentalene ligand is disordered. This confirms the results of a previous spectroscopic 1H NMR study [Katz & Rosenberger (1963). J. Am. Chem. Soc. 85, 2030-2031].
Idioma originalAnglès
Pàgines (de-a)2414-2416
RevistaActa Crystallographica Section C: Crystal Structure Communications
Volum52
Número10
DOIs
Estat de la publicacióPublicada - 15 d’oct. 1996

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